1W2B is a Diffraction, Spectroscopy and Time Resolution beamline and locates at No.15 experimental hall. Originally, it is a Macromolecular Crystallography beam line operating in the 5-18 keV range, with beam spot size of 1mm(H)´0.6mm(V). Recently 1W2B developed the capability of hosting X-ray absorption spectroscopy (XAS) experiments, small-angle X-ray scattering (SAXS) experiments and time resolved experiments. It runs not only in the dedicated mode of synchrotron radiation but also in the parasitic mode.
Transmission XAS with parallel plate ion chamber and fluorescence XAS with Lytle detector is available. Typical time for taking a XAS spectrum is 15 minutes. Quick XAS is also available, which permits several ten seconds minimum to take a spectrum. Advanced self-developed area silicon detector will be equipped in 2018 which will permit spectrum acquisition of much lower concentration samples (approximately several parts per million).
A SAXS system was assembled in June 2016. During the dedicated beam time, we tested the setup of the system and had a trial run. The system began to host users in June 2017. The sample-to-detector distance is adjustable from 0.5 meter to 1.2 meter.
Utilizing laser pump - X-ray probe method, pico-second resolution X-ray absorption spectroscopy and X-ray diffraction method were developed on 1W2B station, which have wide application prospects in photo-chemistry and photo-physics. Ultrafast X-ray absorption spectroscopy began to host users in June 2017.
Supported techniques:
Macromolecular crystallography
Multi-wavelength/Single-wavelength Anomalous Dispersion
Multiple/Single isomorphous replace
Molecular replace
Micromolecule crystallography
X-ray Absorption Fine Structure
Small angle X-ray scattering
Wide angle X-ray scattering
Pico-second resolution X-ray absorption spectroscopy and X-ray diffraction method
Scopes:
Biological Macromolecular
Organic/Inorganic micromolecule
Beamline equipments
Pilatus 1M detector
Ion Chamber and Lytle detector
Time resolved pump-probe system
Mardtb and Mar 165 CCD
Cryogenic Sample Changer(Marresearch, 18 samples)
Oxford cryogenic freezing system
Cold-light source optical microscope
Beamline Specs
Source Wiggler
Energy Range 5-18 keV
Resolution (ΔE/E) better than 4×10-4
Flux (photons/sec) 1012
Beam Size (H×V) 1mm×0.6 mm
